He'd thrown down the gauntlet.
The word is also sometimes applied to a heavy timber fitted with iron spikes or projections to be thrown down upon besiegers, and to the large work known as a "cavalier."
The soap is from this again grained off or salted out, and the underlye so thrown down carries with it coloured impurities which may have been in the materials or which arise from contact with the boiler.
The more northerly of these was partly destroyed by an earthquake (27 B.C.) and the upper part thrown down.
It is now allowed to stand for some time, decanted from any sediment, and finally mixed with the calculated quantity of potassium sulphate (or if ammonium alum is required, with ammonium sulphate), well agitated, and the alum is thrown down as a finely-divided precipitate of alum meal.