The former experiment had been performed by Scheele and Priestley, who had named the gas " phlogisticated air "; Lavoisier subsequently named it oxygen, regarding it as the " acid producer " (OE, sour).
I therefore made an experiment to determine whether the whole of a given portion of the phlogisticated air of the atmosphere could be reduced to nitrous acid, or whether there was not a part of a different nature to the rest which would refuse to undergo that change.
I then, in order to decompound as much as I could of the phlogisticated air [nitrogen] which remained in the tube, added some dephlogisticated air to it and continued the spark until no further diminution took place.
His last chemical paper, published in 1788, on the "Conversion of a mixture of dephlogisticated and phlogisticated air into nitrous acid by the electric spark," describes measures he took to authenticate the truth of the experiment described in the 1785 paper, which had "since been tried by persons of distinguished ability in such pursuits without success."